Aluminium Potassium Sulphate:
Alum BP
Potash Alum BP
Aluminium Potassium Sulphate BP
AlK(SO4)2,12H2O__474.4__7784-24-9
DEFINITION
Content
99.0 per cent to 100.5 per cent of AlK(SO4)2,12H2O.
CHARACTERS
Appearance
Granular powder or colourless, transparent, crystalline masses.
Solubility
Freely soluble in water, very soluble in boiling water, soluble in glycerol, practically insoluble in ethanol (96 per cent).
IDENTIFICATION
A. Solution S (see Tests) gives the reactions of sulphates.
B. Solution S gives the reaction of aluminium.
C. Shake 10 ml of solution S with 0.5 g of sodium bicarbonate R and filter. The filtrate gives reaction (a) of potassium.
TESTS
Solution S
Dissolve 2.5 g in water R and dilute to 50 ml with the same solvent.
Appearance of solution
Solution S is clear and colourless.
pH: 3.0 to 3.5.
Ammonium: Maximum 0.2 per cent.
Iron: Maximum 100 ppm.
Heavy metals: Maximum 20 ppm.
PotassiumAlum USP
Aluminum Potassium Sulfate USP
AlK(SO4)2·12H2O 474.39
Sulfuric acid, aluminum potassium salt (2:1:1), dodecahydrate.
Aluminum potassium sulfate (1:1:2) dodecahydrate [7784-24-9].
Anhydrous 258.21 [10043-67-1].
Potassium Alum contains not less than 99.0 percent and not more than 100.5 percent of AlK(SO4)2, calculated on the dried basis.
Packaging and storage— Preserve in tight containers, and store at room temperature.